Many MIM metal injection molding process,
even if in the industry do a few years, may not be able to understand all
processes have to understand, here, and we share of MIM316L powder injection
process parameter selection problems, mainly include:
1, metal powder how to choose?
Sintered density of PF-3F, PF-5F, PF-10F
and PF-15F four kinds of metal powders at different sintering temperatures. It
can be seen that, at a certain temperature range, the higher the sintering
temperature, the greater the sintering density, which changes little with the
sintering temperature. In a certain range, the larger the size of the powder,
the greater the sintering density. Spherical powder is beneficial to increase
the density of vibration, increase the loading capacity and improve the
sintering density.
2, metal powder and binder ratio?
The viscosity increases with the increase
of the solid content, when the solid content reached 62% after the injection,
the viscosity increased sharply, that the limit of solid content value (maximum
62%).
When the binder is insufficient, there is a
gap between the powder will affect the mechanical strength of the products, the
binder; excessive, solid content is too low, influence of degreasing,
sintering, shrinkage rate.
3, the gate and overflow hole how to choose
the design?
The gate should be higher position in
space, thus reducing the melt feeding in the mold friction, reduce injection
pressure, reduce the possibility of deformation of the products. In addition,
the design of the flash point is also very important, the flash point is used
to cold material loading in injection process, to ensure the uniformity of the
products.
4, C, N and O on the sintering of 316L?
During the sintering process of C, N and O
will have a bad effect on sintering 316L. Carbon has a strong affinity for
chromium, generation of Cr23C6, the grain boundary decreased chromium content
of solid solution, the formation of chromium depleted zone; nitrogen in
stainless steel in the supersaturated solid solution, cooling in the form of
Cr2N in the grain boundaries, thereby reducing the MIM corrosion resistance of
the products; oxygen and chromium can form oxide film Cr2O3, and the liquid
wettability is not good, the influence of liquid flow, hinder the densification
process.
5, how to choose the sintering atmosphere?
This is because in Ar+H2 atmosphere, low
dew point protection powder surface is not oxidized, powder C and O C-O remove
more than 900 DEG C; in vacuum atmosphere, gas gap more easily excluded,
accelerate the densification process; in N2 atmosphere, the dew point is not
low enough, resulting in the oxide film forming powder that is not conducive to
the formation of the sintered parts, hinder the diffusion of atoms.
In addition, in the process of sintering,
the slower heating rate is conducive to the formation of grain boundary rules
and reduce the isolation of obturator, increase sintering time, sintering
density increased slightly, but the decline of the mechanical properties
(grain). The increase of sintering platform at 800 DEG to 1100 DEG C, lower heating
rate is a good choice!
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